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Scientific paper - Original scientific paper
Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone
Croatica Chemica Acta, 57 (1984), 4; 621-628. urn:nbn:hr:163:150895
Matijašić, Ivanka; Andreetti, Giovanni D.; Sgarabotto, Paolo; Bezjak, Aleksandar; Fleš, Dragutin

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Matijašić, I., Andreetti, G. D., Sgarabotto, P., Bezjak, A. & Fleš, D. (1984). Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone. Croatica Chemica Acta, 57. (4), 621-628. Retrieved from https://urn.nsk.hr/urn:nbn:hr:163:150895

Matijašić, Ivanka, et al. "Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone." Croatica Chemica Acta, vol. 57, no. 4, 1984, pp. 621-628. https://urn.nsk.hr/urn:nbn:hr:163:150895

Matijašić, Ivanka, Giovanni D. Andreetti, Paolo Sgarabotto, Aleksandar Bezjak and Dragutin Fleš. "Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone." Croatica Chemica Acta 57, no. 4 (1984): 621-628. https://urn.nsk.hr/urn:nbn:hr:163:150895

Matijašić, I., et al. (1984) 'Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone', Croatica Chemica Acta, 57(4), pp. 621-628. Available at: https://urn.nsk.hr/urn:nbn:hr:163:150895 (Accessed 05 October 2024)

Matijašić I, Andreetti GD, Sgarabotto P, Bezjak A, Fleš D. Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone. Croatica Chemica Acta [Internet]. 1984 [cited 2024 October 05];57(4):621-628. Available at: https://urn.nsk.hr/urn:nbn:hr:163:150895

I. Matijašić, G. D. Andreetti, P. Sgarabotto, A. Bezjak and D. Fleš, "Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone", Croatica Chemica Acta, vol. 57, no. 4, pp. 621-628, 1984. [Online]. Available at: https://urn.nsk.hr/urn:nbn:hr:163:150895. [Accessed: 05 October 2024]

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Metadata
Title (english)Crystal and molecular structure of (S)-a-(p-bromobenzenesulphonamido)-B-propiothiolactone
AuthorIvanka Matijašić
AuthorGiovanni D. Andreetti
AuthorPaolo Sgarabotto
AuthorAleksandar Bezjak
AuthorDragutin Fleš
Author's institutionUniversity of Zagreb
Faculty of Pharmacy and Biochemistry
Scientific / art field,
discipline and subdiscipline		NATURAL SCIENCES
Chemistry
Abstract (english)
(S)-a-(p-Bromobenzenesulphonamido)-{J-propiothiolactone, C9H8N03S2Br, crystallizes in the orthorhombic system with a = = 1.0125(2), b = 1.2439(1) and c = 0.9304(3) nm, Z = 4 in space group P212121• The compound is isostructural with the analogous chloro derivative. The crystal structure has been refined from diffractometer data to conventional R and Ra values of 0.045 and 0.048 for 2277 reflections with I ~ 2a (I). The heterocyclic four-membered ring has a puckering angle of 8.9(4) 0 • The dihedral angle between the best planes of the /)-propiothiolactone and benzene rings is 84.1(2) 0 • The structure consists of discrete molecules connected along the a axis by intermolecular hydrogen bonds N-H ... O of 291.9(7) pm.
Languageenglish
Publication typeScientific paper - Original scientific paper
Publication statusPublished
Peer reviewPeer review - international
Publication versionPublished version
Journal titleCroatica Chemica Acta
Numberingvol. 57, no. 4, pp. 621-628
p-ISSN0011-1643
e-ISSN1334-417X
URN:NBNurn:nbn:hr:163:150895
Publication1984
Document URLhttps://hrcak.srce.hr/194130
Type of resourceText
Access conditionsOpen access
Terms of useLicence In copyright icon
Created on2020-04-30 15:03:00